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Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.

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Some standards require the test sample to be aged prior to testing, to simulate the precipitation that might occur during welding. Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack.

ISO is specifically for duplex and all austenitic stainless steels, and recommends ageing at two different temperatures:. The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid.

ASTM G28 lists alloys and specifies the test ashm for each.

ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results. This specification is for detecting susceptibility to intergranular attack IGA. A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens.

Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance. The test uses a visual inspection of the surface of the bent specimen to determine pass or fail.


Intergranular Corrosion Testing: An Overview of ASTM A262

How do you select the right ASTM corrosion testing method for your material? Some suggested criteria for the listed alloys are shown in Table 2, below. The specifications for bend testing are shown in Table 4. A recent publication on intergranular corrosion.

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Suggested test methods for different corrosion resistant alloys. Where a bend test is required, the sample must be bent over a mandrel of a diameter related to the specimen diameter, without any cracking, as determined by inspection under a low power microscope and a microsection in any suspicious areas.

The latter is a German test, but it is often called up in European projects. Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your sstm while providing actionable results you can rely on.

Intergranular Corrosion Tests for CRAs

At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type. Samples may be rectangular or cylindrical to suit the test vessel, but where a bend test is required, it is suggested that the sample be a minimum of mm long.

Test Samples Samples may be rectangular or cylindrical to suit the test vessel, but where a bend test is required, it is suggested that the sample be a minimum of mm long. Both of these tests should be followed by water quenching. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.


All austenitic stainless steels should meet this requirement, if proper annealing took place. It depends on which Practice is selected, but asstm ranges from to days for different tests.

This document also points out which alloys the tests are intended for, and recommends the most appropriate test when none is specified.

If you are s262 sure, please contact us for assistance. For many alloys, the onset is at 0. Where a standard is included in a purchase specification, this must be followed, although it is advised that unsuitable tests, such as the Huey test for duplex and super austenitic stainless steels, are queried. Methods for preparing the test specimens, rapid screening awtm, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.

This document describes all three of these tests for four common standards, and describes the differences. Where no specific test is specified, Table 5 suggests the 2a62 appropriate alongside a second choice, if the first is declined.

Table 1 below shows the various methods for four common standards: ISO is the most rigorous in terms of defining test methods, and says which alloys should use which asgm methods as follows: This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively.